반응 #305072

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2-(3-methyl-2-oxopiperidin-3-yl)-1H-isoindole-1,3(2H)-dione

3-phtalimidopiperidin-2-one

→

(+/−)2-(2-methoxy-3-methyl-3,4,5,6-tetrahydropyridin -3-yl)-1H-isoindole-1,3(2H)-dione

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후처리

1. 1
   기타prepared by analogy to the method
2. 2
   기타the compound was obtained as a yellow oil

실험 절차

By analogy with the method described in example 1 (step 1.1), using 2-(3-methyl-2-oxopiperidin-3-yl)-1H-isoindole-1,3(2H)-dione (prepared by analogy to the method described in Liebigs Annalen der Chemie (1987), (7), 647-8. Archiv der Pharmazie (Weinheim, Germany) (1989), 322(8), 499-505, (Heterocycles (1996), 42(2), 537-42, Enantiomer (2001), 6(5), 275-279, Synthesis (1991), (5), 417-20)) in place of 3-phtalimidopiperidin-2-one, the compound was obtained as a yellow oil.

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