반응 #2931

반응 방정식

water

1-(3-Furyl)-1-(4-methyl-5-oxazolyl)ethanol

Trimethylsilylazide

boron trifluoride

→

title compound

1-Azido-1-(3-furyl)-1-(4-methyl-5-oxazolyl)ethane

용매

benzene

반응 조건

후처리

1. 1
   추출extracted

실험 절차

1-(3-Furyl)-1-(4-methyl-5-oxazolyl)ethanol (1 g) was suspended in benzene (4 ml). Trimethylsilylazide (822 μl) was added followed by boron trifluoride diethyletherate (770 μl). The mixture was stirred overnight at room temperature, then poured into water and extracted to give the title compound.

출처