반응 #2680

반응 방정식

HCl

tri-n-decylcarbinol

calcium chloride

→

tri-n-decylmethylchloride

수율 90.0%

용매

methylene chloride

반응 조건

후처리

1. 1
   세척The product mixture is then washed with 1 liter of a 10% sodium carbonate solution
2. 2
   건조The organic layer is dried with magnesium sulfate
3. 3
   기타the methylene chloride evaporated off

실험 절차

One mole of tri-n-decylcarbinol was added to a mixture of 0.2 liters of methylene chloride and 0.32 moles calcium chloride. Approximately 1.5 moles of HCl gas was slowly bubbled through the solution. The product mixture is then washed with 1 liter of a 10% sodium carbonate solution. The organic layer is dried with magnesium sulfate and the methylene chloride evaporated off to give a 90% yield of tri-n-decylmethylchloride.

출처