반응 #2676

반응 방정식

alcohol

2,3-dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-styrol

m-chloro perbenzoic acid

→

expected product

수율 99.6%

2,3-dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-(1,2-epoxy) styrol

수율 99.6%

용매

AcOEt cyclohexane

cyclo-hexane ethyl acetate

반응 조건

후처리

1. 1
   기타were reacted

실험 절차

Using the procedure of Stage D of Example 40, 13.2 g of thee allylic alcohol of Step C and 10.3 g of m-chloro perbenzoic acid were reacted to obtain 13.7 g of the expected product with a Rf=0.25 (AcOEt-cyclohexane 6-4).

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