반응 #2675

반응 방정식

ester

2,3-dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-styryl carboxylate

diisobutylaluminium hydride

→

expected product

수율 99.6%

2,3-dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-styrol

수율 99.6%

반응 조건

후처리

1. 1
   기타were reacted

실험 절차

Using the procedure of Stage C of Example 40, 20 g of ester of Step B and 88 ml of diisobutylaluminium hydride were reacted to obtain 17.9 g of the expected product melting at 60° C.

출처