반응 #2522

ord-20a899a14e114ac08ae516cd5bce4b60

반응 방정식

Nc1ccccc1
aniline
O=C(O)c1ccc([N+](=O)[O-])cc1
4-nitrobenzoic acid
O=C(Nc1ccccc1)c1ccc([N+](=O)[O-])cc1
title compound
수율 97.5%
O=C(Nc1ccccc1)c1ccc([N+](=O)[O-])cc1
4-Nitro-N-(phenyl)benzamide
수율 97.5%

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Using aniline (1.50 ml, 16.5 mmol) and 4-nitrobenzoic acid (1.77 g, 10.5 mmol), the procedure of Reference Example 16 was repeated to obtain 2.48 g (97.5%) of the title compound in the form of colorless powder.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05728835uspto-grants-1998_03