반응 #2510562
ord-e927ec18400f4fb68541b3cfdd6578e9
반응 방정식
L-isopulegol
hydrogen
→
L-menthol
시약
없음
반응 조건
온도
80°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타to 75° C
실험 절차
Example 1 was repeated using L-isopulegol with a purity of 99.9% by weight and 99.8% ee, which was introduced at a rate of 12.6 g/h (total amount 303 g) into the reactor at a hydrogen pressure of 40 bar. The main reactor (MR) was heated to 80° C., the postreactor to 75° C. L-menthol (99.8% ee) was obtained in an amount of 306 g corresponding to a rate of 12.8 g/h. The chemical purity of the L-menthol output is compiled in Table 2.