반응 #2508

ord-884108655568491b9b7065118f5c820d

반응 방정식

N#Cc1ccccc1N
2-aminobenzonitrile
COc1ccc(S(=O)(=O)Cl)cc1
4-methoxybenzenesulfonyl chloride
COc1ccc(S(=O)(=O)Nc2ccccc2C#N)cc1
title compound
수율 63.7%
COc1ccc(S(=O)(=O)Nc2ccccc2C#N)cc1
N-(2-Cyanophenyl)-4-methoxybenzenesulfonamide
수율 63.7%

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Using 2-aminobenzonitrile (1.03 g, 8.55 mmol) and 4-methoxybenzenesulfonyl chloride (1.78 g, 8.55 mmol), the procedure of Reference Example 2 was repeated to obtain 1.57 g (63.7%) of the title compound in the form of colorless solid.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05728835uspto-grants-1998_03