반응 #2507846

ord-98c3198f70774fed8176f88e3b49eb54

반응 방정식

O.O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
trehalose dihydrate
NCC(=O)O
glycine
CC(C[*:1])[*:2]
polypropylene
→
NCC(=O)O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
Trehalose Glycine

반응물

O.O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
trehalose dihydrate
NCC(=O)O
glycine
CC(C[*:1])[*:2]
polypropylene

시약

없음

용매

O
water
O
water

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    workup.ADDITIONwas added at room temperature
  2. 2
    기타was obtained
  3. 3
    workup.ADDITIONWithout adding any acid

실험 절차

17.84 g of trehalose dihydrate and 4.03 g of glycine were carefully weighed and transferred into a sterile polypropylene bottle, to which 300 ml of purified water was added at room temperature and stirred slowly until a clear solution was obtained. The pH was measured and found to be 5.5. Without adding any acid, the volume was adjusted to 350 ml with purified water. The pH was measured and found to be 5.5.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07956028B2uspto-grants-2011_06