반응 #2507809

반응 방정식

pentacene

maleimide

→

pentacene maleimide

용매

dichlorobenzene

반응 조건

후처리

1. 1
   온도The mixture is cooled to room temperature
2. 2
   여과the precipitate is filtered
3. 3
   세척washed with toluene
4. 4
   기타dried
5. 5
   기타Recrystallization from dichlorobenzene

실험 절차

A suspension of pentacene (287 mg, 1 mmole) and maleimide (1 mmole) in 4 mL of dichlorobenzene is heated to 160° C. for 4 hours. The mixture is cooled to room temperature and the precipitate is filtered, washed with toluene and dried. Recrystallization from dichlorobenzene affords pure samples of pentacene-maleimide adduct as white needles.

출처