반응 #2507

ord-f25119feab274c18843fec44487e7f9a

반응 방정식

COc1cccc(N)c1
m-anisidine
COc1ccc(S(=O)(=O)Cl)cc1
4-methoxybenzenesulfonyl chloride
COc1ccc(S(=O)(=O)Nc2cccc(OC)c2)cc1
title compound
수율 99.7%
COc1ccc(S(=O)(=O)Nc2cccc(OC)c2)cc1
4-Methoxy-N-(3-methoxyphenyl)benzenesulfonamide
수율 99.7%

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Using m-anisidine (0.99 ml, 8.55 mmol) and 4-methoxybenzenesulfonyl chloride (1.78 g, 8.55 mmol), the procedure of Reference Example 2 was repeated to obtain 2.50 g (99.7%) of the title compound in the form of light yellow oil.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05728835uspto-grants-1998_03