반응 #2504

ord-80f67fcb3ee14ef2b196db2ad72d47b4

반응 방정식

COc1ccccc1N
o-anisidine
COc1ccc(S(=O)(=O)Cl)cc1
4-methoxybenzenesulfonyl chloride
COc1ccc(S(=O)(=O)Nc2ccccc2OC)cc1
title compound
수율 90.1%
COc1ccc(S(=O)(=O)Nc2ccccc2OC)cc1
4-Methoxy-N-(2-methoxyphenyl)benzenesulfonamide
수율 90.1%

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Using o-anisidine (1.0 ml, 8.55 mmol) and 4-methoxybenzenesulfonyl chloride (1.78 g, 8.55 mmol), the procedure of Reference Example 2 was repeated to obtain 2.26 g (90.1%) of the title compound in the form of colorless powder.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05728835uspto-grants-1998_03