반응 #2501394

반응 방정식

2,4,6,8-tetramethylcyclotetrasiloxane

benzene

2-hydroxyethyl acrylate

→

title compound

Ethylene Glycol 2,4,6,8-tetramethylcyclotetrasiloxanyl Ether Acrylate

용매

water

반응 조건

후처리

1. 1
   기타The organic layer was separated
2. 2
   세척washed with 200 mL of cold water
3. 3
   건조dried over MgSO4
4. 4
   여과filtered
5. 5
   농축concentrated by distillation

실험 절차

To a solution containing 1M of 2,4,6,8-tetramethylcyclotetrasiloxane and 0.01 g of (CH3CO2)2Zn was slowly added 1M of 2-hydroxyethyl acrylate. The resulting mixture was stirred for 12 hours at a room temperature. Thereafter, 200 mL of benzene and 200 mL of cold water were added. The organic layer was separated, washed with 200 mL of cold water, dried over MgSO4, filtered and concentrated by distillation to provide the title compound of Formula 1A (yield: 97%).

출처