반응 #2492107

ord-d8ca5378e37241f889b9114146451930

반응 방정식

Nc1ccc(S(=O)(=O)[O-])c2ccccc12.[Na+]
naphthionic acid sodium salt
Nc1ccc(S(=O)(=O)O)c2ccccc12
Naphthionic Acid

시약

없음

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타Slowly add hydrochloric acid, and white precipitation
  2. 2
    workup.STIRRINGStir the slurry for at least 4 hours
  3. 3
    여과filter the slurry

실험 절차

In a large beaker, add naphthionic acid sodium salt and water and stir to complete solution, pH=9.2-9.4. Slowly add hydrochloric acid, and white precipitation occurs at pH=2.2-2.4. Stir the slurry for at least 4 hours, then filter the slurry. Use the wetcake in Stage 2.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08802829B2uspto-grants-2014_08