반응 #2484856
ord-bae2a6957965486d905a0c1e072beae2
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1여과the reaction mixture was filtered
- 2추출extracted with ether
- 3기타Evaporation
실험 절차
A solution of 35.2 gm (0.2 mol) of α-ethyl cinnamic acid in 450 ml of 3% sodium hydroxide was reduced in a hydrogen atmosphere at 60 psi using 4 gm of 5% palladium on charcoal. After hydrogen uptake had ceased, the reaction mixture was filtered, acidified with hydrochloric acid and extracted with ether. Evaporation gave 36 gm (0.2 mol) of 2-benzyl butanoic acid.