반응 #2482120

ord-4c1ec2bcaa5b475f9759e36bc5507d2d

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    온도the mixture is refluxed for 1 hour
  2. 2
    농축After concentrating

실험 절차

To 2-methyl-3,4,6-trifluorobenzoic acid (3.2 g) is added thionyl chloride (7 ml) and the mixture is refluxed for 1 hour. After concentrating, 2-methyl-3,4,6-trifluorobenzoyl chloride (3.3 g) is obtained.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05811576uspto-grants-1998_09