반응 #2482
ord-9263fd3c38db4e7d8af1acf74087dcb3
반응 방정식
용매
반응 조건
온도
90°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도Heating for an additional hour at 135° C.
실험 절차
The apparatus of Example 2 was charged with 17.1 grams (0.1 mol) of ethyl 3-(N-vinylformamido)propionate, 6.2 grams (0.1 mol) of ethylene glycol, and 0.15 gram of 25% sodium methoxide in methanol solution. The mixture was stirred at 90° C. for 2 hours. No evolution of ethanol was observed during the reaction period. Heating for an additional hour at 135° C. also failed to generate a volatile coproduct which indicated no conversion to the desired product.