반응 #2479878

ord-91e8c78440314a209782ee3b072a0f3c

반응 방정식

C1=C(c2cc3ccccc3[nH]2)Cc2ccccc21
2-(2indenyl)indole
CCOC(=O)/C=C\C#N
ethyl cis-β-cyanoacrylate
O=C1C=CC2=Nc3ccccc3C2=C1
6-oxo carbazole

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

In Method B (FIG. 2), a 2-(heteroaryl)indole derivative (1-3), or 2-(aryl)indole derivative such as 2-(2indenyl)indole 4 is reacted with ethyl cis-β-cyanoacrylate in the presence of a catalyst such as SnCl4, AlCl3, EtAlCl2, Et2AlCl or TFA in CH2 Cl2, C2H4Cl2 or toluene as solvent to give the 6-oxo carbazole compounds of formula I of the invention.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05801190uspto-grants-1998_09