반응 #2467931

ord-805213d305c74b3da5b5bcfb7dfd9ad1

반응 방정식

[Na+].[OH-]
sodium hydroxide
Nc1nc(N)nc(N)n1
melamine
COC(C=O)OC
dimethoxyethanal
COC(C=O)OC.Nc1nc(N)nc(N)n1
Melamine Dimethoxyethanal

반응 조건

온도
52.5°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    온도This mixture was heated
  2. 2
    온도while maintaining the pH
  3. 3
    기타close to 9-9.5 with adjustment

실험 절차

200 g of melamine (1.59 mol) were added to 580 g of a 60% aqueous solution of dimethoxyethanal (3.35 mol). This mixture was heated under stirring for 2 h at 50-55° C. while maintaining the pH close to 9-9.5 with adjustment, if necessary, with as much 20% sodium hydroxide as was required (about 7 g).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08257832B2uspto-grants-2012_09