반응 #2439927

ord-ec4a51e12237403a8ab1b826d2c0eb6d

반응 방정식

O=[N+]([O-])[O-].O=[N+]([O-])[O-].[Zn+2]
zinc nitrate
O=P([O-])([O-])[O-].[Na+].[Na+].[Na+]
sodium phosphate
O=P([O-])([O-])[O-].O=P([O-])([O-])[O-].[Zn+2].[Zn+2].[Zn+2]
zinc phosphate

시약

없음

반응 조건

온도
80°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타to allow precipitates
  2. 2
    기타to be produced
  3. 3
    기타Centrifugal separation (2000 ppm, for 5 min)
  4. 4
    세척washing with water

실험 절차

0.1 M zinc nitrate and 1 M monobasic sodium phosphate were mixed while stirring to allow precipitates to be produced by heating at 80° C. twice. Centrifugal separation (2000 ppm, for 5 min) and washing with water were repeated five times to produce a zinc phosphate paste. The zinc phosphate paste was adjusted to give a solid content concentration of 20 parts by weight and to include methyldiethanolamine at 1 part by weight, and dispersion was made similarly to Example 1. The treatment liquid for surface conditioning was obtained by preparing it from the resulting concentrated dispersion liquid, in a similar manner to Example 1.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07749319B2uspto-grants-2010_07