반응 #2392492

반응 방정식

hydrazino-acetaldehyd diethylacetal

methylisothiocyanate

→

2-(2,2-diethoxy-ethyl)-4-methyl-thiosemicarbazide

용매

ethanol

반응 조건

후처리

1. 1
   기타the solvent is evaporated off

실험 절차

A mixture of 4 g of hydrazino-acetaldehyd diethylacetal in 40 ml of ethanol is stirred with 1.97 g of methylisothiocyanate for ca. 4 hours at room temperature, the solvent is evaporated off and 2-(2,2-diethoxy-ethyl)-4-methyl-thiosemicarbazide is obtained in crystalline form.

출처