반응 #2389089

반응 방정식

dodecane thiol

sulfuryl chloride

→

dodecansulfenyl chloride

용매

CHCl3

반응 조건

후처리

1. 1
   기타Removal of solvent (aspirator)

실험 절차

To a solution of dodecane thiol (1.00 mL, 4.17 mmol, Aldrich Chemical Company) in 20 mL CHCl3 was added sulfuryl chloride (0.74 mL, 9.18 mmol, Aldrich Chemical Company), and the resulting mixture was stirred at room temperature for 18 h. Removal of solvent (aspirator), afforded dodecansulfenyl chloride that was determined to be sufficiently pure by 1H NMR.

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