반응 #2389088

반응 방정식

dodecane thiol

chloride

→

dodecansulfenyl chloride

용매

CHCl3

반응 조건

후처리

1. 1
   기타Removal of solvent (aspirator)

실험 절차

To a solution of dodecane thiol (1.00 mL, 4.17 mmol, Aldrich) in 20 mL CHCl3 was added suliryl chloride (0.74 mL, 9.19 mmol, Aldrich), and the regulting mixture was stirred at room temperature for 18 h. Removal of solvent (aspirator), afforded dodecansulfenyl chloride that was determined to be sufficiently pure by 1H NMR.

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