반응 #2389085

반응 방정식

9-Hydroxyphenalenone

aluminum chloride

→

Tris (9-oxidophenalenone) aluminum

용매

toluene

반응 조건

후처리

1. 1
   기타to form
2. 2
   온도The flask was then cooled
3. 3
   여과the contents filtered

실험 절차

9-Hydroxyphenalenone (1.5 g) was placed in a 100 mL round-bottom flask. Dry toluene (50 mL) was added to the flask together with aluminum chloride (0.113 g). The solution turned yellow-orange, and a precipitate began to form. The mixture was refluxed at 110° C. overnight. The flask was then cooled and the contents filtered. Crude yield 1.69 g, mp>300° C.

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