반응 #2383780

ord-418306255f36449a96863edfa193ae18

반응 방정식

O=C(O)c1ccccc1
Benzoic acid
C=COCCCl
2-chloroethyl vinyl ether
[Na+].[OH-]
sodium hydroxide
CCN(CC)CC
triethylamine
C=COCCOC(=O)c1ccccc1
Benzoyloxyethyl Vinyl Ether

용매

반응 조건

온도
120°CELSIUS
상세 조건
See reaction.notes.procedure_details.

실험 절차

Benzoic acid (244 g) (2 mol) was dissolved in 3,000 ml of toluene, and thereto were added 320 g of 2-chloroethyl vinyl ether, 88 g of sodium hydroxide, 25 g of tetrabutylammonium bromide, and 100 g of triethylamine. The resulting mixture was stirred with heating at 120° C. for 5 hours.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06489080B2uspto-grants-2002_12