반응 #2383779

반응 방정식

Pentafluorobenzenesulfonyl chloride

tetramethylammonium hydroxide

→

pentafluorobenzenesulfonic acid tetramethylammonium salt

용매

methanol

반응 조건

후처리

1. 1
   온도cooling

실험 절차

Pentafluorobenzenesulfonyl chloride (25 g) was dissolved in 100 ml of methanol with ice-cooling, and 100 g of a 25% aqueous solution of tetramethylammonium hydroxide was gradually added thereto. The reaction mixture was stirred at room temperature for 3 hours, thereby a solution of a pentafluorobenzenesulfonic acid tetramethylammonium salt was obtained. This solution was used for salt exchange of a sulfonium salt and an iodonium salt.

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