반응 #2383764

반응 방정식

4-chloro-3-methylpyrazole

formalin

→

solid

수율 95.0%

N-hydroxymethyl-4-chloro-3-methylpyrazole

수율 95.0%

용매

methanol

반응 조건

후처리

1. 1
   기타Water and methanol were then evaporated

실험 절차

116 g (1.0 mol) of 4-chloro-3-methylpyrazole in 50 ml of methanol were dissolved in 100 g (1.0 mol) of formalin solution (30%) at room temperature. Water and methanol were then evaporated. The title compound remained as a white solid (yield 95%).

출처