반응 #2380638

반응 방정식

1-[2-(S)-amino-4-methylpentyl ]-L-proline 4-phenylbutylamide

9-fluorenone-4-carbonyl chloride

→

title compound

수율 18.0%

1-[2-(S)-[(9-Oxo-9H-fluorene-4-carbonyl)amino]-4-methylpentyl]-L-proline 4-Phenylbutylamide

수율 18.0%

반응 조건

실험 절차

Using the procedure described in Example 7, treatment of 1-[2-(S)-amino-4-methylpentyl ]-L-proline 4-phenylbutylamide (134 mg) with 9-fluorenone-4-carbonyl chloride (131 mg) provided 35 mg(18%) of the title compound. The 1H NMR and Mass spectrum analysis of this compound was consistent with the structure.

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