반응 #2373414

반응 방정식

1-(2',4'-dichlorophenyl)-2-(1,2,4-triazol-1-yl)-ethyl allyl ether

nitric acid

→

1-(2',4'-dichlorophenyl)-2-(1,2,4-triazol-1-yl)-ethyl allyl ether nitrate

수율 95.0%

용매

chloroform

반응 조건

후처리

1. 1
   기타The crystallization of the salt
2. 2
   workup.ADDITIONby adding 250 ml of ether
3. 3
   여과After filtering off
4. 4
   기타drying

실험 절차

29.5 g (0.1 mole) of 1-(2',4'-dichlorophenyl)-2-(1,2,4-triazol-1-yl)-ethyl allyl ether were dissolved in 200 ml of chloroform and 6.4 g of 95% strength nitric acid were added. The crystallization of the salt was completed by adding 250 ml of ether. After filtering off and drying, 34 g (95% of theory) of 1-(2',4'-dichlorophenyl)-2-(1,2,4-triazol-1-yl)-ethyl allyl ether nitrate of melting point 131° C. were obtained.

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