반응 #2358553

ord-2cf4a8c7dc0241a78461beff640a1035

반응 방정식

O.O.O.O.O.O.O.O.O.O=[N+]([O-])[O-].O=[N+]([O-])[O-].O=[N+]([O-])[O-].[Al+3]
aluminum nitrate nonahydrate
O=[N+]([O-])[O-].O=[N+]([O-])[O-].[Mg+2]
magnesium nitrate
O=[N+]([O-])O
nitric acid
→
O=[N+]([O-])[O-].O=[N+]([O-])[O-].O=[N+]([O-])[O-].[Al+3]
aluminum nitrate
O=[N+]([O-])[O-].O=[N+]([O-])[O-].[Mg+2]
magnesium nitrate

반응물

O.O.O.O.O.O.O.O.O.O=[N+]([O-])[O-].O=[N+]([O-])[O-].O=[N+]([O-])[O-].[Al+3]
aluminum nitrate nonahydrate
O=[N+]([O-])[O-].O=[N+]([O-])[O-].[Mg+2]
magnesium nitrate
O=[N+]([O-])O
nitric acid

시약

없음

용매

O
water

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타was prepared
  2. 2
    workup.ADDITIONThe aqueous solution was gradually added dropwise to 10.0 kg of a silica sol solution (trade name “Snowtex N-30” manufactured by Nissan Chemical Industries Ltd., SiO2 content: 30% by mass)
  3. 3
    기타kept at 15° C.

실험 절차

An aqueous solution of 2.0 kg of aluminum nitrate nonahydrate, 1.5 kg of magnesium nitrate and 0.27 kg of 60% nitric acid dissolved in 3.0 L of pure water was prepared. The aqueous solution was gradually added dropwise to 10.0 kg of a silica sol solution (trade name “Snowtex N-30” manufactured by Nissan Chemical Industries Ltd., SiO2 content: 30% by mass) kept at 15° C. with stirring and having a colloidal particle size of 10 to 20 nm, so as to give a mixed slurry of a silica sol, aluminum nitrate and magnesium nitrate. Thereafter, the mixed slurry was kept at 50° C. for 24 hours for aging. The aged mixed slurry was cooled to room temperature and was spray dried with a spray dryer with an outlet temperature set to 130° C. to obtain a dried substance.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US09120085B2uspto-grants-2015_09