반응 #2358451

반응 방정식

thionyl chloride

2-methyl-3,4,6-trifluorobenzoic acid

→

2-methyl-3,4,6-trifluorobenzoyl chloride

반응 조건

후처리

1. 1
   온도by heating
2. 2
   온도refluxing for 1 hour
3. 3
   농축The reaction mixture was concentrated

실험 절차

7 ml of thionyl chloride was added to 3.2 g of 2-methyl-3,4,6-trifluorobenzoic acid, followed by heating and refluxing for 1 hour. The reaction mixture was concentrated, giving 3.3 g of 2-methyl-3,4,6-trifluorobenzoyl chloride. Then 5 ml of toluene was added to the resulting 2-methyl-3,4,6-trifluorobenzoyl chloride to give a toluene solution.

출처