반응 #2320104
ord-3e3e36bfa43f4b0691fec661b4d2f193
반응 방정식
4-bromo-1,2-dichlorobenzene
cis-2,6-dimethyl-1-propyl-piperazine
HCl
→
cis-4-(3,4-dichloro-phenyl)-2,6-dimethyl-1-propyl-piperazine
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타the title compound was recovered by the procedure
- 2기타described in Preparation 9
실험 절차
Beginning with 4-bromo-1,2-dichlorobenzene and cis-2,6-dimethyl-1-propyl-piperazine, the title compound was recovered by the procedure described in Preparation 9: m.p. 225° C. (HCl), MS m/z (rel. intensity, 70 eV)) 301 (M+, 24), 271 (64), 112 (bp), 70 (47), 56 (53).