반응 #2306

반응 방정식

Oxalyl chloride

4-((4-pyridyl)piperazin-1-yl)benzoic acid

→

4-[(4-pyridyl)piperazin-1-yl]benzoyl chloride

용매

dichloromethane

반응 조건

후처리

1. 1
   기타evaporated to dryness

실험 절차

Oxalyl chloride (0.5 ml) was added to a stirred suspension of 4-((4-pyridyl)piperazin-1-yl)benzoic acid in dichloromethane (15 ml), followed by DMF (1 drop). The mixture was stirred for 2 hours and evaporated to dryness to give 4-[(4-pyridyl)piperazin-1-yl]benzoyl chloride which was used immediately.

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