반응 #2298632

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2,5-diethyl-4-methyl-1,6-dihydro-6-pyrimidone

4-[2-bromoethoxy]benzaldehyde

NaH

→

title compound

수율 28.0%

4-[2-[2,5-Diethyl-4-methyl-6-oxo-1,6-dihydro-1-pyrimidinyl]ethoxy]benzaldehyde

수율 28.0%

반응 조건

후처리

1. 1
   기타that described in preparation 1

실험 절차

The title compound (1.42 g, 28%) was prepared from 2,5-diethyl-4-methyl-1,6-dihydro-6-pyrimidone (2.70 g, 16.26 mmol) and 4-[2-bromoethoxy]benzaldehyde (4.09 g, 17.86 mmol) in the presence of 95% NaH (508 mg, 20 mmol) as base by a similar procedure to that described in preparation 1.

출처