반응 #2275688
ord-3f67295fdaca46fca78f9eca296a8f09
반응 방정식
Acetic acid 3-acetoxy-2-tert-butoxycarbonylamino-propyl ester
trifluoroacetic acid
→
product
2-Acetoxy-1-acetoxymethyl-ethyl-ammonium trifluoroacetate
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타when the volatiles were removed at reduced pressure
실험 절차
Acetic acid 3-acetoxy-2-tert-butoxycarbonylamino-propyl ester (7.2 g) was dissolved in trifluoroacetic acid (40 ml) and stirred at ambient temperature. Effervescence was rapid at the start and had stopped after 1 h when the volatiles were removed at reduced pressure to give the product as a viscous oil in quantitative yield.