반응 #2267055
ord-1a1a3434cae245c49c2a39443e27ee10
반응 방정식
pentafluorobenzenesulfonyl chloride
tetramethylammonium hydroxide
→
tetramethylammonium pentafluorobenzenesulfonate
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도cooling
실험 절차
25 gof pentafluorobenzenesulfonyl chloride was dissolved in 100 ml of methanol under ice-cooling. Then 100 g of a 25% aqueous solution of tetramethylammonium hydroxide was slowly added thereto. By stirring at room temperature for 3 hours, a solution of tetramethylammonium pentafluorobenzenesulfonate was obtained. Thus solution was employed in salt exchange between sulfonium salt and iodonium salt.