반응 #2206330

ord-73cd9074ae0f4fae901c53070d2b4bfd

반응 방정식

C[C@H](O)[C@H](O)[C@@H](O)[C@@H](O)C=O
L-rhamnose
CCCCCCCCCCCCCCCCCCN
stearylamine
→
CCCCCCCCCCCCCCCCCCNC1O[C@@H](C)[C@H](O)[C@@H](O)[C@H]1O
N-Octadecyl-L-rhamnopyranosylamine

반응물

C[C@H](O)[C@H](O)[C@@H](O)[C@@H](O)C=O
L-rhamnose
CCCCCCCCCCCCCCCCCCN
stearylamine

시약

없음

용매

CC(C)O
2-propanol
O
water

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타had resulted
  2. 2
    여과the crystals were filtered off with suction
  3. 3
    세척washed with ethanol and ether
  4. 4
    기타dried in vacuo

실험 절차

9 g of L-rhamnose and 13.5 g of stearylamine in 100 ml of 2-propanol and 50 ml of water were stirred at 50° C. until a clear solution had resulted. After 50 hours at room temperature, the crystals were filtered off with suction, washed with ethanol and ether and dried in vacuo. Yield: 17.4 g.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04683222uspto-grants-1987_07