반응 #220552

ord-031830ddfdf148619ff48c3996b411fd

반응 방정식

O=C(O)Cc1ccc(Br)cc1
4-bromophenylacetic acid
CCC(N)C(=O)OCC(C)C
iso-butyl 2-aminobutyrate
CCC(NC(=O)Cc1ccc(Br)cc1)C(=O)OCC(C)C
title compound
CCC(NC(=O)Cc1ccc(Br)cc1)C(=O)OCC(C)C
2-[(4-bromophenyl)acetamido]butyric acid iso-butyl ester

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The reaction was monitored by tlc on silica gel and purification
  2. 2
    여과was by filtration

실험 절차

Following General Procedure BI above and using 4-bromophenylacetic acid (Aldrich) and iso-butyl 2-aminobutyrate (prepared following General Procedure BJ above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07390801B2uspto-grants-2008_06