반응 #2200579
ord-1c63baaa7b784e589ea1319894e1fcf4
반응 방정식
ethyl 4-chloro-3-hydroxybutyrate
DMCS
→
Ethyl 4-Chloroacetoacetate
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타was carried out at 150° C
실험 절차
The quantitation of ethyl 4-chloro-3-hydroxybutyrate was carried out by gas chromatography. Thus, using a glass column (ID 3 mm×1 m) packed with PEG-20M Chromosorb WAW DMCS 10%, 80/100 mesh (product of GL Sciences Inc.), chromatography was carried out at 150° C. The detection was made by FID.