반응 #219192

반응 방정식

1-chloro-3-(triphenylphosphanylidene)-propane-2-one

benzaldehyde

→

title compound

1-Chloro-4-phenyl-but-3-en-2-one

용매

toluene

반응 조건

후처리

1. 1
   온도is heated
2. 2
   온도at reflux for 20 hours
3. 3
   기타Evaporation to dryness
4. 4
   기타yields a mixture

실험 절차

A mixture of 1-chloro-3-(triphenylphosphanylidene)-propane-2-one (2.8 g, 7.9 mmol) and freshly distilled benzaldehyde (0.7 g, 6.6 mmol) in toluene (10 ml) is heated at reflux for 20 hours. Evaporation to dryness yields a mixture containing the title compound that is used in the subsequent step without purification.

출처