반응 #2189991

반응 방정식

2-amino-5-nitrobenzothiazole

benzoyl chloride

pyridine

→

N-(5-nitrobenzothiazol-2-yl)benzamide

수율 78.5%

용매

water

반응 조건

후처리

1. 1
   기타the resulting precipitate was separated by filtration

실험 절차

A mixture of 2-amino-5-nitrobenzothiazole (1.52 g, 7.8 mmol), benzoyl chloride (1.36 mL, 11.7 mmol) and pyridine (15 mL) was heated to 60° C. for 24 h. The mixture was poured into water (250 mL), and the resulting precipitate was separated by filtration to yield N-(5-nitrobenzothiazol-2-yl)benzamide (1:83 g, 6.12 mmol, 78%) as a yellow solid.

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