반응 #2186214
ord-585b503ec23d472ca3706a5b2c3f1a68
반응 방정식
phenacyl bromide
tetrahydrothiophene
water
diethyl ether
→
Phenacyltetrahydrothiophenium Bromide
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타separated into two layers
실험 절차
88.2 g (0.44 mole) of phenacyl bromide and 39.1 g (0.44 mole) of tetrahydrothiophene were dissolved in 220 g of nitromethane, which was stirred for 4 hours at room temperature. 800 g of water and 400 g of diethyl ether were added to the reaction solution whereupon the mixture separated into two layers. The aqueous layer was taken out, which was an aqueous solution of the target compound, phenacyltetrahydrothiophenium bromide.