반응 #2186190
ord-20136f727d9549e5991771cb70f0576e
반응 방정식
thioanisole
dimethyl sulfate
water
→
dimethylphenylsulfonium hydrogen sulfate
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타separated into two layers
실험 절차
6.2 g (0.05 mole) of thioanisole and 6.9 g (0.055 mole) of dimethyl sulfate were stirred for 12 hours at room temperature. 100 g of water and 50 ml of diethyl ether were added to the reaction solution whereupon the mixture separated into two layers. The aqueous layer was taken out, which was an aqueous solution of the target compound, dimethylphenylsulfonium hydrogen sulfate.