반응 #218252

반응 방정식

dichloro(β-cyano)ethoxyphosphine

diisopropylethylamine

diisopropylamine

→

Diisopropylaminochloro(β-cyano)ethoxyphosphine

용매

dichloromethane

반응 조건

후처리

1. 1
   기타The reaction by mixture
2. 2
   기타the reaction mixture is ready for next step reaction

실험 절차

To a solution of 1.9 mL (1 3.8 mmol) of dichloro(β-cyano)ethoxyphosphine in 40 mL of dichloromethane cooled in an ice-water bath was added 10 mL of diisopropylethylamine, followed by adding 2.3 mL (13.8 mmol) of diisopropylamine under Argon. The reaction by mixture was warmed up to room temperature and stirred for 2 h. After adding 0.1 gm of DMAP into the solution, the reaction mixture is ready for next step reaction.

출처