반응 #2175479

반응 방정식

1,3-dioxan-2-one

benzoyl peroxide

hexafluoropropene

→

4-(1,1,2,3,3,3-hexafluoropropyl)-1,3-dioxan-2-one

반응 조건

후처리

1. 1
   기타Example 6 was prepared
2. 2
   온도The reactor was maintained at the set temperature for an additional 24 h
3. 3
   기타The reactor contents were collected

실험 절차

Example 6 was prepared by combining 1,3-dioxan-2-one (240 g, 2.35 moles) (Richman Chemical Inc., Lower Gwynedd, Pa.) with benzoyl peroxide (5 g, 0.02 moles) in a 600 mL Parr reactor. The reactor was heated to 73° C. and hexafluoropropene (16 g, 0.1066 moles) was fed into the reactor over a 2 h period. The reactor was maintained at the set temperature for an additional 24 h. The reactor contents were collected and analyzed by GC/MS.

출처