반응 #217480
ord-ed593dcb2091417f8386ebc40775ec71
반응 방정식
2-acetylnaphthalene
ethyl heptafluorobutyrate
→
4,4,5,5,6,6,6-Heptafluoro-1-(2-naphthyl)-1,3-hexanedione
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타The compound was synthesized
- 2기타The product was crystallized from petroleum ether
실험 절차
The compound was synthesized according to example 1 using 2-acetylnaphthalene and ethyl heptafluorobutyrate as starting materials. The product was crystallized from petroleum ether. 1H NMR (CDCl3): 6.76 (s, 1 H); 7.57-7.66 (m, 2H); 7.90 (bd, 1 H); 7.93-7.94 (m, 2H); 7.98 (bd, 1 H); 8.53 (s, 1H). IR (film): 1602 (C═O); 1232 (C—F).