반응 #217479
ord-38bd0544e87d4ca6b596713afa8114c1
반응 방정식
2-acetylnaphthalene
ethyl pentafluoropropionate
→
4,4,5,5,5-Pentafluoro-1-(2-naphthyl)-1,3-pentanedione
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타The compound was synthesized
- 2기타The product was crystallized from petroleum ether
실험 절차
The compound was synthesized according to example 1 using 2-acetylnaphthalene and ethyl pentafluoropropionate as starting materials. The product was crystallized from petroleum ether. 1H NMR (CDCl3): 6.79 (s, 1 H); 7.57-7.67 (m, 2H); 7.90 (bd, 1 H); 7.94-7.95 (m, 2H); 7.99 (bd, 1H); 8.53 (s, 1 H). IR (film): 1602 (C═O); 1201 (C—F).