반응 #2161007
ord-f0b5cf29340c457d9e4d29e41e7b1ee0
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1농축concentrated
실험 절차
A solution of 5.8 g (30.5 mmol) of 2,4,5-trifluoro-6-methylbenzoic acid, 4.7 g (37.0 mmol) of oxalyl chloride, and 100 ml of dichloromethane was treated with three drops of DMF. The reaction mixture was stirred at room temperature for two hours, then concentrated to give 6.3 g of the title compound as an oily solid. The product was used "as is" in the next step.