반응 #215767

반응 방정식

2-Methoxy-4-(1-acetyl-4-piperidyloxy)benzoic acid

thionyl chloride

→

2-methoxy-4-(1-acetyl-4-piperidyloxy)benzoyl chloride

용매

THF

반응 조건

후처리

1. 1
   농축concentrated in vacuo

실험 절차

2-Methoxy-4-(1-acetyl-4-piperidyloxy)benzoic acid (0.546 g, 1.86 mmol) in THF (10 ml) was stirred under nitrogen and treated with thionyl chloride (0.27 ml, 0.44 g, 3.7 mmol). The mixture was stirred at ambient temperature for 18 hours, then concentrated in vacuo to give 2-methoxy-4-(1-acetyl-4-piperidyloxy)benzoyl chloride.

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