반응 #215231

반응 방정식

2,2-dimethyl-11-n-hexyl-11-amino-undeca-4,8-dienal-oxime

4 Pa

3,3-dimethyl-12-n-hexyl-1-aza-1,5,9-cyclododecatriene

hydroxylamine sulfate

hydrochloric acid

→

1-n-Hexyl-10,10-dimethyl-1,11-diaminoundecane

용매

water

반응 조건

실험 절차

Reaction of 3,3-dimethyl-12-n-hexyl-1-aza-1,5,9-cyclododecatriene with hydroxylamine sulfate, in the presence of hydrochloric acid and water, to 2,2-dimethyl-11-n-hexyl-11-amino-undeca-4,8-dienal-oxime, and hydrogenation of this to given 1-n-hexyl-10,10-dimethyl-1,10-diaminoundecane; b.p. 135° C./4 Pa; nD20 =1.4624.

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